NIH, National Cancer Institute, Division of Cancer Treatment and Diagnosis (DCTD) NIH - National Institutes of Health National Cancer Institute DCTD - Division of Cancer Treatment and Diagnosis

Effect of ischemic time, fixation time, and fixative type on HER2/neu immunohistochemical and fluorescence in situ hybridization results in breast cancer.

Author(s): Moatamed NA, Nanjangud G, Pucci R, Lowe A, Shintaku IP, Shapourifar-Tehrani S, Rao N, Lu DY, Apple SK

Publication: Am J Clin Pathol, 2011, Vol. 136, Page 754-61

PubMed ID: 22031314 PubMed Review Paper? No

Purpose of Paper

The purpose of this paper was to determine the effects of fixation parameters on the evaluation of human epidermal growth factor 2 (HER2) status of breast cancer specimens.

Conclusion of Paper

Delaying fixation by 4 days did not effect determination of HER2 status by immunohistochemistry (IHC) and fluorescent in situ hybridization (FISH). The most consistent IHC results were obtained from specimens fixed with Pen-FIX for 1-168 h, or 10% neutral buffered formalin (NBF) for more than 72 h. The most consistent FISH results were obtained from specimens fixed in 10% NBF for 1-168 h, or Pen-Fix, Sakura molecular fixative (SMF), or zinc formalin for 7 h or less.

Studies

  1. Study Purpose

    The purpose of this study was to determine the effects of fixation parameters on the evaluation of HER2 status in breast cancer specimens by IHC. A portion of a single grade 3 invasive ductal carcinoma was fixed in 10% NBF for 12 h, and the remainder was stored for 4 days at 4 degrees C prior to fixation for 0-168 h in each of the tested fixatives. IHC staining was performed using the HercepTest and was scored using the American society of clinical oncologists (ASCO)/ College of American pathologists (CAP) guidelines.

    Summary of Findings:

    In the specimen that was immediately fixed in 10% NBF for 12 h the IHC score was 3+ and. The authors report that the 4 days of cold ischemia time at 4 degrees C prior to fixation did not impact IHC results or quality of morphology. The most consistent results were obtained when the specimen was fixed with Pen-FIX resulting in scores of 3+ for all fixation times (1-168 h). When the specimens were fixed in 10% NBF, fixation for 1 h yielded a HER2 score of 1+, and fixation for 2-48 h led to variable scores of 2+ or 3+, but fixation for 72 h or longer resulted in consistent HER2 scores of 3+. Fixation in 15% NBF, SMF, and zinc formalin generally led to a HER2 score of 3+, but specimens fixed in 15% NBF for 10-24 h, SMF for 1 or 12 h, or zinc formalin for 1, 24 or 168 h scored 2+. Fixation in Bouin's fixative for 1 h led to a HER2 score of 1+, and longer fixation times led to scores of 2+ or 3+ with equal frequency and no trends were observed.

    Biospecimens
    Preservative Types
    • Formalin
    • Other Preservative
    • None (Fresh)
    Diagnoses:
    • Neoplastic - Carcinoma
    Platform:
    AnalyteTechnology Platform
    Protein Immunohistochemistry
    Morphology H-and-E microscopy
    Pre-analytical Factors:
    ClassificationPre-analytical FactorValue(s)
    Biospecimen Preservation Type of fixation/preservation Bouin's fixative
    Formalin (buffered)
    None (fresh)
    Pen-fix
    Sakura molecular fixative
    Zinc formalin
    Biospecimen Preservation Time in fixative 0 h
    1 h
    2 h
    3 h
    4 h
    5 h
    6 h
    7 h
    8 h
    9 h
    10 h
    11 h
    12 h
    24 h
    48 h
    72 h
    168 h
    Immunohistochemistry Specific Targeted peptide/protein HER2
    Biospecimen Acquisition Cold ischemia time < 1 h
    4 days
    Biospecimen Preservation Concentration of fixative 10% NBF
    15% NBF
  2. Study Purpose

    The purpose of this study was to determine the effects of fixation parameters on the assessment of HER2 status of breast cancer specimens by FISH. A portion of a single grade 3 invasive ductal carcinoma was fixed in 10% NBF for 12 h and the remainder was stored for 4 days at 4 degrees C prior to fixation for 0-168 h in each of the tested fixatives. A HER2/chromosome enumeration probe 17 (CEP17) ratio of greater than 2.2 was defined as positive.

    Summary of Findings:

    In all specimens showing successful hybridization, the HER2/CEP17 ratio was greater than 7.8 which was observed in the specimen fixed immediately in 10% NBF for 12 h. Successful FISH hybridization was observed in all specimens fixed in 10% NBF, regardless of fixation duration, and in specimens fixed in 15% NBF for 1-9 h or 12-168 h. FISH hybridization was also successful in all specimens fixed for 7 h or less in Pen-Fix, SMF, or zinc formalin, but specimens fixed for longer than 7 h in these three fixatives often showed no hybridization. The single specimen fixed for 1 h in Bouin's fixative yielded successful hybridization, but specimens fixed in Bouin's for longer than 1 h failed to hybridize. No hybridization was observed in the unfixed specimen.

    Biospecimens
    Preservative Types
    • Formalin
    • None (Fresh)
    Diagnoses:
    • Neoplastic - Carcinoma
    Platform:
    AnalyteTechnology Platform
    DNA FISH
    Pre-analytical Factors:
    ClassificationPre-analytical FactorValue(s)
    Biospecimen Acquisition Cold ischemia time < 1 h
    4 days
    Biospecimen Preservation Type of fixation/preservation Bouin's fixative
    Formalin (buffered)
    None (fresh)
    Pen-fix
    Sakura molecular fixative
    Zinc formalin
    Biospecimen Preservation Time in fixative 0 h
    1 h
    2 h
    3 h
    4 h
    5 h
    6 h
    7 h
    8 h
    9 h
    10 h
    11 h
    12 h
    24 h
    48 h
    72 h
    168
    FISH Specific Targeted nucleic acid HER2/neu
    Biospecimen Preservation Concentration of fixative 10% NBF
    15% NBF

You Recently Viewed  

News and Announcements

  • Most Downloaded SOPs in 2024

  • New Articles on the GTEx Project are Now FREELY Available!

  • Just Published!

  • More...