NIH, National Cancer Institute, Division of Cancer Treatment and Diagnosis (DCTD) NIH - National Institutes of Health National Cancer Institute DCTD - Division of Cancer Treatment and Diagnosis

Controlled storage conditions prolong stability of biochemical components in whole blood.

Author(s): Stahl M, Brandslund I

Publication: Clin Chem Lab Med, 2005, Vol. 43, Page 210-5

PubMed ID: 15843219 PubMed Review Paper? No

Purpose of Paper

The purpose of this paper was to determine the effects of centrifugation speed and storage prior to centrifugation on clinical chemistry analytes in plasma.

Conclusion of Paper

Potassium and phosphate were affected by storage of whole blood at 20 degrees C for 8 h or more, prior to centrifugation, but no other analytes were affected. Centrifugation speed had no effects on the 7 analytes evaluated in this paper.

Studies

  1. Study Purpose

    The purpose of this study was to determine the effects of centrifugation at 1200 x g versus 3000 x g on 7 clinical chemistry analytes in plasma. After centrifugation, plasma was refrigerated at 4 degrees C until analysis.

    Summary of Findings:

    Centrifugation speed had no effects on albumin, calcium, glucose, lactate dehydrogenase, potassium, sodium or total protein in plasma.

    Biospecimens
    Preservative Types
    • Other Preservative
    Diagnoses:
    • Not specified
    Platform:
    AnalyteTechnology Platform
    Carbohydrate Clinical chemistry/auto analyzer
    Electrolyte/Metal Clinical chemistry/auto analyzer
    Small molecule Clinical chemistry/auto analyzer
    Protein Clinical chemistry/auto analyzer
    Pre-analytical Factors:
    ClassificationPre-analytical FactorValue(s)
    Biospecimen Aliquots and Components Centrifugation Multiple speeds compared
  2. Study Purpose

    The purpose of this study was to determine the effects of delayed centrifugation on 27 clinical chemistry analytes in plasma. After centrifugation, plasma was stored at 4 degrees C until analysis.

    Summary of Findings:

    Potassium increased with increasing delays to centrifugation at 17 or 20 degrees C and decreased with increasing delays to centrifugation at 23 or 25 degrees C. However, when specimens were held at 20 degrees C, prior to centrifugation, the change in potassium was clinically irrelevant until at least an 8 h delay. Plasma phosphate decreased when blood was stored at 20 degrees C for 8 h or more before centrifugation. No other clinically relevant effects of delayed centrifugation were observed.

    Biospecimens
    Preservative Types
    • Other Preservative
    Diagnoses:
    • Not specified
    Platform:
    AnalyteTechnology Platform
    Carbohydrate Clinical chemistry/auto analyzer
    Electrolyte/Metal Clinical chemistry/auto analyzer
    Glycoprotein Clinical chemistry/auto analyzer
    Steroid Clinical chemistry/auto analyzer
    Small molecule Clinical chemistry/auto analyzer
    Peptide Clinical chemistry/auto analyzer
    Protein Clinical chemistry/auto analyzer
    Pre-analytical Factors:
    ClassificationPre-analytical FactorValue(s)
    Storage Storage duration 0 h
    2 h
    4 h
    6 h
    8 h
    10 h
    12 h
    Storage Storage temperature 17 degrees C
    20 degrees C
    23 degrees C
    25 degrees C
    Biospecimen Aliquots and Components Centrifugation Centrifugation delays investigated

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