NIH, National Cancer Institute, Division of Cancer Treatment and Diagnosis (DCTD) NIH - National Institutes of Health National Cancer Institute DCTD - Division of Cancer Treatment and Diagnosis

RNA extraction from archival formalin-fixed paraffin-embedded tissue: a comparison of manual, semiautomated, and fully automated purification methods.

Author(s): Bohmann K, Hennig G, Rogel U, Poremba C, Mueller BM, Fritz P, Stoerkel S, Schaefer KL

Publication: Clin Chem, 2009, Vol. 55, Page 1719-27

PubMed ID: 19617290 PubMed Review Paper? No

Purpose of Paper

The purpose of this paper was to compare RNA yield and quantification of breast cancer biomarkers in RNA extracted from formalin fixed paraffin embedded (FFPE) breast tumors by 4 different methods.

Conclusion of Paper

All 4 extraction methods allowed for extraction of RNA in all specimens; however, the average RNA yield was highest from the EZI RNA tissue MiniKit (Qiagen; method 3). All four kits produced two clusters of cycle threshold (CT) values with the highest CT values (lowest yield) being from specimens that were 20 years old. When breast cancer marker genes were examined, the normalized values between methods were much better correlated than the CTs indicating normalized expression was a robust marker. While method 3 had the best yield, the fully automated method using VERSANT kPCR (method 1) gave the most reproducible results making it the method of choice.

Studies

  1. Study Purpose

    The purpose of this study was to determine the effects of specimen age and extraction method on RNA yield and quantification from FFPE breast tumor specimens.

    Summary of Findings:

    Real-time PCR amplification was possible in all specimens which had been fully extracted. Using CT values as an indicator of yield, method 3 (CT=22.7) performed the best followed by the RNeasy FFPE kit (method 4)( CT=22.8), the manual VERSANT kPCR with extra centrifugation (method 2)(CT=22.9) and method 1 (CT=23.3). All methods produced two clusters of CT values. The higher CT group (lower yield) corresponded to specimens that were 20 years old. Within this group, method 4 had a substantially lower RNA yield. When breast cancer marker genes were examined, the normalized values between methods were much better correlated than the CTs. While method 3 had the best yield, method 1 gave the most reproducible results making it the method of choice.

    Biospecimens
    Preservative Types
    • Formalin
    Diagnoses:
    • Neoplastic - Carcinoma
    Platform:
    AnalyteTechnology Platform
    RNA Real-time qRT-PCR
    Pre-analytical Factors:
    ClassificationPre-analytical FactorValue(s)
    Storage Storage duration 3 years
    5 years
    20 years
    Analyte Extraction and Purification Analyte isolation method Automated VERSANT kPCR molecular system (Siemens Healthcare)
    Manual VERSANT kPCR with extra centrifugation molecular system (Siemens Healthcare)
    EZI RNA tissue Minikit (Qiagen)
    RNeasy FFPE kit (Qiagen)

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